Chapter 1 Experimental Research Method of Chemical Engineering Principle 5 1.1 Dimensional analysis 5 1.2 Mathematical model method 7 1.3 The direct experiment method 9 1.4 Cold-model experiment method 10
Chapter 2 Experiment of Chemical Engineering Principle 11 Experiment 1 Reynolds experiment 11 Experiment 2 Bernoulli equation experiment 14 Experiment 3 Comprehensive experiment of fluid mechanics 18 Experiment 3.1 Determination of the pipeline fluid resistance 19 Experiment 3.2 Calibration of orifice meter and Venturi meter 27 Experiment 3.3 Determination of the centrifugal pump performance curve 32 Experiment 4 Determination of the characteristic curves of a centrifugal pump 33 Experiment 5 Comprehensive experiment of convective heat transfer 45 Experiment 6 Comprehensive experiment on the measurement of heat transfer coefficient K of heat exchanger 56 Experiment 7 Plate column distillation experiment 59 Experiment 8 Packed column distillation experiment 72 Experiment 9 Determination of fluid mechanics of plate column 75 Experiment 10 Absorption-desorption experiment 81 Experiment 11 Drying experiment 89 Experiment 12 Fluidized bed drying experiment 96 Experiment 13 Extraction experiment 103 Experiment 14 Pervaporation membrane experiment 107 Experiment 15 Ultrafiltration membrane separation experiment 111
Chapter 3 Methods of Processing Experimental Data 113 3.1 Significant digits and operation rules 113 3.2 Error analysis of experimental data 114 3.3 Experimental data processing 116 3.4 Representation of experimental data with mathematical equation 123
Chapter 4 Common Measuring Instrument in Laboratory 132 4.1 Pressure measurement 132 4.2 Metering of fluids 139 4.3 Temperature measurement 153
Appendix 166 Appendix 1 SXK-2 type high precision flow integrator 166 Appendix 2 ZW5433 three-phase digital meter 168 Appendix 3 Instructions for hydrostatic balance 170 Appendix 3.1 Specific gravity table of ethanol solution 172 Appendix 3.2 Density table of water 175 Appendix 4 Abbe refractometer 175 Appendix 4.1 Relationship between refractive index of ethanol-propanol and solution concentration 178 Appendix 4.2 Relationship between composition and refractive index of n-heptane-methyl cyclohexane system 178 Appendix 5 Gas-liquid equilibrium data 179 Appendix 5.1 Gas-liquid equilibrium data of ethanol-aqueous solution at atmospheric pressure（P = 760mmHg） 179 Appendix 5.2 Gas-liquid equilibrium data of ethanol-propanol at atmospheric pressure（molar fraction） 179 Appendix 5.3 Gas-liquid equilibrium data of n-heptane methyl cyclohexane at atmospheric pressure 180 Appendix 6 Characteristic parameters of the four packings 180 Appendix 7 Oxygen dissolving instrument 180 Appendix 8 752-model spectrophotometer 182 Appendix 9 Principles of automatic acquisition of computer data and automatic control 184 Appendix 10 Installation and operation instructions of“Chemical Engineering Principle Experiment CAI” 185 Appendix 11 Data recording and collation table of unit operation experiment 195 Appendix 11.1 Data recording and collation table of Reynolds experiment 195 Appendix 11.2 Data recording and collation table of Bernoulli equation experiment 195 Appendix 11.3 Data recording and collation table of the pipeline fluid resistance determination 196 Appendix 11.4 Data recording and collation table of calibration experiment of orifice and Venturi flowmeter 197 Appendix 11.5 Data recording and collation table of determination of centrifugal pump characteristic curve 198 Appendix 11.6 Data recording and collation table of comprehensive heat transfer experiment 199 Appendix 11.7 Data recording and collation table of comprehensive experiment of heat transfer coefficient K measurement 200 Appendix 11.8 Data recording and collation table of plate column distillation experiment 201 Appendix 11.9 Data recording and collation table of packed column distillation experiment 201 Appendix 11.10 Data recording and collation table of determination of hydromechanical properties of plate column 202 Appendix 11.11 Data recording and collation table of absorption-desorption experiment 202 Appendix 11.12 Data recording and collation table of drying experiment 204 Appendix 11.13 Data recording and collation table of the fluidized bed drying experiment 205 Appendix 11.14 Data recording and collation table of extraction experiment 206 Appendix 11.15 Data recording and collation table of pervaporation membrane experiment 207 Appendix 11.16 Data recording and collation table of ultrafiltration membrane separation experiment 208
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