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全新正版现货农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs 9787122349194 庞国芳著化学工业出版社

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作者: 庞国芳著
出版社: 化学工业出版社
ISBN: 9787122349194

出版时间: 2019-11
装帧: 精装
开本: 16开

作者: 庞国芳著
出版社: 化学工业出版社

ISBN: 9787122349194
出版时间: 2019-11

装帧: 精装
开本: 16开

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前言
Food safety is a major security issue necessary to ensure the sound development of human society. The widespread use of pesticides, veterinary drugs, and other agricultural chemicals have contributed to widespread contamination in agricultural products. The long-term consumption of food with high residues of pesticides and veterinary drugs will cause both acute and chronic toxicity in humans and induce resistant strains, thus resulting in allergies, cancer, mutation, and teratogenicity. In order to ensure human health and food safety,countries all over the world have issued strict food safety and hygiene standards. The People’s Republic of China (PRC) has implemented strict monitoring of pesticide and veterinary drug residues, such as maximum residue limits for veterinary drugs in food of animal origin (Announcement No. 235 of the Ministry of Agriculture of the People’s Republic of China) and national food safety standards: Maximum residue limits for pesticides in food (GB 2763- 2016). The commonly used pesticides and veterinary drugs approved in China and the main agricultural products of urban residents’ daily consumption are almost all covered.

The book is a systematic summary of the high-throughput chromatographymass spectrometry technique for the analysis of multipesticides, veterinary drugs, and other agricultural chemical residues in agriculture products of plant and animal origin. Its technical characteristics are mainly embodied in the simultaneous determination of hundreds of compounds, as well as low cost and high efficiency.

This book is divided into two volumes. In Volume 1, pesticides and related chemicals are selected as the main research object, while gas chromatographymass spectrometry (GC-MS), gas chromatography-tandem mass spectrometry (GC-MS-MS), and liquid chromatography-tandem mass spectrometry (LC-MSMS) are concerned. This volume includes more than 20 analytical methods for the high-throughput analysis of multipesticide residues, and more than 1000 pesticides and related chemicals in more than 10 kinds of agricultural products and drinking water can be detected, and 400–500 kinds of pesticide residues can be detected simultaneously with the pretreatment undertaken just once. The methods for the analysis of 793 pesticides and related chemical residues in foods of plant origin applicable to fruit juices, vegetable juices, fruit wines, fruits, vegetables, cereals, tea, Chinese medicinal herbs (ramulus mori, honeysuckle, Chinese wolfberry, and lotus leaf), and edible fungi (mushroom) are introduced in Part 1; the methods for the analysis of 790 pesticides and related chemical residues in foods of animal origin applicable to honey, milk, milk powder, aquatic products (globefish, eel, and prawn), and animal muscle tissues are presented in Part 2; while the methods for the analysis of 450 pesticides and related chemical residues in drinking water are introduced in Part 3. Furthermore, the three major parameter databases adopted in the analysis of more than 1000 pesticides and related chemicals are also included in this volume: ①chromatography-mass spectrometry characteristic parameters include retention time, quantitative and qualitative ions, fragment voltage and collision energy, etc.;②performance parameters of the methods include linear equation, linear range and correlation coefficient, etc.; and③gel permeation chromatography (GPC) purification analysis parameters.

In Volume 2, the methods for the analysis of 20 species (nearly 200 kinds) of veterinary drug residues in edible animal tissues (muscle, liver, kidney, and fat), dairies (milk and milk powder), bee products (honey, royal jelly, and its lyophilized powder), aquatic products (globefish, eel, and roasted eel) and animal urine are selected as main subjects of study. The 65 analytical methods for the analysis of multiveterinary drug residues are described in different chapters by category (sulfonamides, β-adrenergic agonists, aminoglycosides, chloramphenicols,β-lactams, macrolides, nitrofurans, anabolic steroids, nonsteroidal anabolic steroids, glucocorticoids, fluoroquinolones, tetracyclines, sedatives, pyrazolones, quinoxalines, nitromidazoles, benzimidazoles, levamisole, thiourea pyrimidines, and polyethers), and 90% of the methods are LC-MS-MS. Meanwhile the physical and chemical properties, efficacy, side effects, and maximum allowable residual limit of all the compounds are also provided.

In short, this book is the summary of the work of the author team who, for more than 20 years, engaged in the research and practice of detection technology of pesticides and veterinary drug residues. These methods for the analysis of pesticides and veterinary drugs are innovative research results based on the international frontier of pesticides and veterinary drug residue analysis, and the analytical techniques adopted are new technologies widely concerned in the field of residue analysis in the world today. The performance indexes of the methods can meet the requirements of the Codex Alimentarius Commission and the world’s major developed countries; meanwhile the methods are in conformity with the developing trend of international residue analysis and they are advanced in the world. In addition, the methods established in this book have become the current effective national standard methods in China and they can be used as the detection basis of relevant testing institutions and the law basis of the relevant government departments. Nevertheless, due to the limitations of the level, there may be unavoidable errors. We would kindly ask the users of this publication to provide feedback to the authors so that subsequent editions may be improved upon.

Guo-Fang Pang

导语摘要
本书是《农药兽药多组分残留质谱分析技术》的第2卷兽药篇，介绍了65项适用于动物组织（肌肉、肝脏、肾脏和脂肪）、乳制品（牛奶和奶粉）、蜂产品（蜂蜜、蜂王浆及冻干粉）、水产品（河豚鱼、鳗鱼和烤鳗）及动物尿液中20类兽药残留LC-MS/MS分析方法。方法灵敏度和准确度高，可满足欧盟、日本、国际食品法典委员会（CAC）和美国等限量要求。各章按兽药类别，分别介绍了磺胺类、β-受体激动剂类、氨基糖苷类、氯霉素类、β-内酰胺类、大环内酯类和林可胺类、硝基呋喃类代谢物、甾体类同化激素、非甾类同化激素类、糖皮质激素类、氟喹诺酮类、四环素类、镇静剂类、吡唑酮类、喹啉类、硝基咪唑类、苯并咪唑类、咪唑并噻唑类、硫脲嘧啶类、聚醚类等20类兽药的前处理技术和测定方法，并介绍了兽药的理化性质、代谢和毒理及*残留限量等。本书可供从事食品安全、农业环境保护及农药开发利用等技术研究与应用的技术人员参考，也可作为大学教学参考用书。

作者简介
庞国芳，中国检验检疫科学研究院，研究员，中国工程院院士，国家质检总局首席研究员、国际公职化学家联合会（AOAC）专家，国际AOAC 2014年度 Harvey W. Wiley 奖获得者。近30年一直工作在食品检验检疫一线，致力于食品科学检测技术理论与实践的研究，解决了我国相关出口食品、农产品等遭遇的技术瓶颈，为推动我国对外贸易发展做出了杰出贡献。研究制定了141项国际、国家检测技术标准。在国内、国际出版食品安全检测技术论著10部。发表论文100余篇，35篇被SCI收录。3次荣获国家科学技术进步二等奖，6次荣获国际AOAC组织颁发的科学技术奖励。

目录
Main Researchers/Editors xxvii

Preface xxix

Brief Introduction xxxi

1. Sulfonamides 1

1.1 Curative Effects and Side Effects of Sulfonamides 1

1.2 Chemical Structures and Maximum Residue Limits for Sulfonamide Drugs 2

1.3 Determination of 16 Sulfonamide Residues in Livestock and Poultry Muscles—LC-MS-MS Method (GB/T 20759-2006) 8

1.3.1 Scope 8

1.3.2 Principle 8

1.3.3 Reagents and Materials 8

1.3.4 Apparatus 9

1.3.5 Sample Pretreatment 9

1.3.6 Determination 9

1.3.7 Precision 10

1.3.8 Recovery 12

Researchers 12

Further Reading 16

1.4 Determination of 16 Sulfonamide Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22966-2008) 16

1.4.1 Scope 16

1.4.2 Principle 16

1.4.3 Reagents and Materials 17

1.4.4 Apparatus 17

1.4.5 Sample Pretreatment 18

1.4.6 Determination 18

1.4.7 Precision 19

1.4.8 Recovery 28

Researchers 28

1.5 Determination of 18 Sulfonamide Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22951-2008) 29

1.5.1 Scope 29

1.5.2 Principle 29

1.5.3 Reagents and Materials 29

1.5.4 Apparatus 30

1.5.5 Sample Pretreatment 31

1.5.6 Determination 31

1.5.7 Precision 35

1.5.8 Recovery 36

Researchers 40

1.6 Determination of 8 Sulfonamides residues in Honey—LC-FLD Method (GB/T 18932.5-2002) 41

1.6.1 Scope 41

1.6.2 Principle 41

1.6.3 Reagents and Materials 41

1.6.4 Apparatus 42

1.6.5 Sample Pretreatment 42

1.6.6 Determination 43

1.6.7 Precision 43

1.6.8 Recovery 46

Researchers 47

Further Reading 47

1.7 Determination of 16 Sulfonamide Residues in Honey—LC-MS-MS Method (GB/T 18932.17-2003) 47

1.7.1 Scope 47

1.7.2 Principle 47

1.7.3 Reagents and Materials 48

1.7.4 Apparatus 48

1.7.5 Sample Pretreatment 48

1.7.6 Determination 49

1.7.7 Precision 52

1.7.8 Recovery 52

Researchers 55

Further Reading 55

1.8 Determination of 18 Sulfonamide Residues in Royal Jelly—LC-MS-MS Method (GB/T 22947-2008) 56

1.8.1 Scope 56

1.8.2 Principle 56

1.8.3 Reagents and Materials 56

1.8.4 Apparatus 57

1.8.5 Sample Pretreatment 58

1.8.6 Determination 58

1.8.7 Precision 62

1.8.8 Recovery 64

Researchers 66

2. β-Adrenoceptor Agonists 67

2.1 Determination of 12 β-Agonist Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22965-2008) 67

2.1.1 Scope 67

2.1.2 Principle 67

2.1.3 Reagents and Materials 68

2.1.4 Apparatus 69

2.1.5 Sample Pretreatment 69

2.1.6 Determination 70

2.1.7 Precision 76

2.1.8 Recovery 76

Researchers 78

Further Reading 78

2.2 Determination of 12 β-Agonist Residues in Fugu, E
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全新正版现货 农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs 9787122349194 庞国芳 著 化学工业出版社

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全新正版现货农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs 9787122349194 庞国芳著化学工业出版社